[c#] Argument Exception "Item with Same Key has already been added"

That Exception is thrown if there is already a key in the dictionary when you try to add the new one.

There must be more than one line in rct3Lines with the same first word. You can't have 2 entries in the same dictionary with the same key.

You need to decide what you want to happen if the key already exists - if you want to just update the value where the key exists you can simply

rct3Features[items[0]]=items[1]

but, if not you may want to test if the key already exists with:

if(rect3Features.ContainsKey(items[0]))
{
    //Do something
} 
else 
{
    //Do something else
}

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